Appearance and colour

Colorless, Clear Liquid Without Mechanical Impurities

Solubility in water

Fully Soluble, Solution Is Clear

Mass portion of acetic acid,%,not less than

99,5

Mass portion of acetic aldehyde,%,not more than

0,004

Mass portion of formic acid,%, not more than

0,05

Sulfate (SO 4 ) 3 ,%, not more than

0,0003

Chloride (Cl) mass portion,%,not more than

0,0004

Heavy metals mass portion precipitable ith hydrogen sulfide (Pb),%,not more than

0,004

Mass portion of iron (Fe),%, not more than

0,0004

Nonvolatile residue mass portion,%, not more than

0,004

Stability of potassium permanganate solution colour, min, not more than

60

Mass portion of the substances oxidized by potassium bichromate, cm of sodium thiosulfate solution of concentration with (Na 2 SO 3 *5H 2 O) =0,1 mol/dm 3 (0,1h), not more than

5,0

Appearance

transparent liquid without suspended particles

visual

Acrylonitrile, ppm, not more than

500

Chomatographic Sohajo ACEN-5

Hydrogen cyanide, ppm, not more than

10

ACSA-CV

Water, % wt, not more than

0,15

ASTM 1364-87

Free ammonia, ppm, not more than

5

CCSM TLB 22x

Iron, ppm, not, more than

0,2

DSA-1051-XI

Copper, ppm, not more than

0,2

DSA-1051-XVIII

Colour, Pt-Co scale units, not more than

5

ACSA-C-I

Acetonitrile, % wt, not less than

99,5

RL-LB-6 By Difference *

Appearance

Colorless, transparent liquid without suspended particles

VisualDSA 105

Acetone, ppm, not more than

80

Chromatograph sohajo ACPN-1

Acetonitrile, ppm, not more than

110

Sohajo ACPN-2

Acroleine, ppm, not more than

5

Sohajo ACPN-3

Acidity, as acetic acid, ppm, not more than

35

ASTM D 1613-96

Hydrogen cyanide, ppm, not more than

5

ACSA C-VI

Copper content, ppm, not higher than

0,2

DSA-1051-XVIII

Iron content, ppm, not higher than

0,2

DSA-1051-XI

Water, % wt, not more than

0,4

ASTM D 1364-95

Perohides, ppm, not more than

0,2

Sohajo ACPN-XVII

Colour, Pt-Co scale units, not more than

5

ACSA-C-I

Inhibitor, MENQ, ppm

30-50

DSA-1051-XIX-A

Aniline Oil

99.90

Cyclohexylamine

%wt

0.000

0.010

Cyclohexanol

%wt

0.001

0.010

Nitrobenzene

%wt

0.00020

0.00050

Water

%wt

0.05

0.10

Hydrocarbons(C6)

%wt

<0.002

0.002

Colour

Hazen

<100

100

Crystallization Point

o C

>-6.3

-6.3

Appearance

Flakes

Colour

Light grey to grey

Mass content summed up Naphthols counting on 2 Naphthol 99.1% Min

Mass content Of 1 - Naphthol - 0.03% Max

Melting Point 120.2 Deg C min

n-Butyl Acetate

99.2 percent by weight, minimum

1B-ES-01

Relative density

0.880 to 0.883 at 20/20 o C
This is equivalent to a density of 0.878 to 0.881 g/ml at 20 o C

1B-ES-02

Water

0.03 per cent by weight, medium

1B-ES-03

Acidity

0.005 per cent by weight, medium

1B-ES-04

n-Butanol

0.5 per cent by weight, medium

1B-ES-01

Appearance

clear liquid, free from suspended matter

1B-ES-05

Colour

10 platinum/cobalt, maximum

1B-ES-06

The product meets also the following which will not determined on a routine basis is guaranteed by process control.

Residue on evaporation

0.002 per cent by weight, maximum

1B-ES-07

Distallation
(101.31.pa)

• Initial boiling point
• Dry point

• 124.0 o C, minimum
• 128.0 o C, maximum

Appearance

Transparent colorles liquid

Color in Platinum - Cobalt scale, max

10

Density at 20 o C, g/cm 3 min

0.809 - 0.811

Fraction of total mass of main substance, %min

99.4

Fraction of total mass of acids in terms of acetic acid, %max

0.003

Bromine value gmBR/ 100gm of butanol, max

0.02

Fraction of total mass of nonvolatile matter, %max

0.0025

Mass content of carbonil compounds in terms of oil aldehyde, %max

0.06

Fraction of total mass of moisture, % max

0.08

Appearance

White flakes, light colour allowed

Caustic soda content, min, % by mass

98.5

Sodium carbonate, no more than,% by mass

0.8

Sodium Chloride, no more than, % by mass

0.05

Iron content as per Fe 203, max, % by mass

0.004

Sum of mass fraction of iron and aluminum oxides, %,no more than

0.02

Mass fraction of silicic acid recalculated to SiO2,%,no more than

0.02

Mass fraction of Sodium sulfate,% no more than

0.03

Mass fraction of calcium & magnesium recalculated to calcium, %, no more than

0.01

Mass fraction of sodium chlorate,%,no more than

0.01

Sum of mass fraction of heavy metals precipitated by H2S recalculated to Pb,%,no more than

0.01

Mass fraction of mercury, %, no more than

0.0005

Sodium Hydroxide(Net)

Wt%/ 49.0~51.0 Min./49.5`50.1

Sodium Carbondate,

Wt%/0.2Max/0.1

Sodium Chloride

Wt%/1.1.Max?0.95

Iron

PPM/20 Max/10~15

Sodium Sulfate

Wt%/0.025 Max/0.015

NaOH

Wt%

48.5 Min

Na2CO3

Wt%

0.4 Max

NaCl

Wt.ppm

20 Max

Na2SO4

Wt.ppm

15 Max

Al203

Wt.ppm

10 Max

Fe203

Wt.ppm

6 Max

SiO2

Wt.ppm

5 Max

CaO

Wt.ppm

10 Max

Sp.Gr.@

--

1.515 Min

15.6 Deg C

1.520 Max

Appearance

Gray-Violet crystal/ prills

Main substance

Assay 99.5%

Nonvolatile matter

0.03 % Max.

Chlorine & bromine (as CI)

0.010 % Max.

Sulphate

0.010 % Max

Plumbum (Pb)

1.0mg / Kg

Iron (Fe)

15.0 mg / Kg

Strontium

7.0 mg / Kg

Copper(Cu)

1.0 mg / Kg

Zinc (Zn)

5.0 mg / Kg

Arsenic (As)

0.2 mg / Kg

Hydragyrum (Hg)

0.005 mg / Kg

Mass portion of cyclohexanone, %. min

99,8

Mass portion of impurities, %, max

0,1

Mass portion of water, % max

0,1

Color APHA

Max 20

Specific Gravity 20/20C

0.986(+)(-)3

Acid Value KOH mg/g

Max 0.02

Estre Value

287(+)(-)3

Refroctive Index
Nd20 25C

1.485(+)(-)0.003

Heat Loss

Max0.07

Volume Resistivity 30 C

Min 4.0 x 10 times 11

Synonyme

Acetic Acid, Ethyloster Acetic Ether, Acetoxyethame

Formula

C 4 H 8 O 2

Molecular

88

Shipping Name

Ethyl Acetate

Code/Label

Flammable Liquid, Class 3

Hazardous Waste ID No

5

U N No

1173

Chemical Identity

Description

Clear, Colourless

Odour

Characteristic

Solubility

Freely Soluble in alcohol and acetone

Relative on Evaporation % by mass (Max)

0.01

Acidity( as Acetic Acid) % by mass (Max)

0.01

Ester content ( as Ethyl Acetate ) % by mass (Min)

99.8%

Distillation Range

(a) Initial boiling Point at 760 mm Hg(Min)

76.0 o C

(b) Dry Point at 760 mm Hg(max)

78.5 o C

Water content % by mass (Max)

0.03

H3 PO4

65%Min

SO 4

0.5%Max

Fe( total)

Less than 0.2%

CL

Less than 0.1%

F

Less than 2%

AL 0

0.01%

Density in 60 F

More than 1.47

Cao

Less than 0.1%

Suspended solids

Less than 0.1%

Appearance

Transparent colorless liquid

Color in Platinum- Cobalt scale, max.

7

Density at 20 0 C, g/cm 3 min.

0.801-0.803

Fraction of total mass of main substance, %, min.

99.3

Fraction of total mass of acids in terms of acetic acid, %, max.

0.003

Bromine value gm Br/ 100gm of butanol, max.

0.02

Appearance

Colour Transparent Liquid Without Insoluble Admixtures

Density 20/4 g/sm sq

0.791-0.792

Miscibility with Water

Mixes up with Water without traces of Turbidity and Opalescence

Temperature Limits

a) A limit of boiling, degrees C

64. 0 - 85.5

b) 99% of the product is overtaken in limits, degrees C no more than, %

0.8

Mass content of water, no more, %

0.10%

Mass content of free acids converted to ant pussycat, %, no more than

0.0015

Mass content of aldehydes and ketons in ecalculation on acetone %, no more than

0.003

Mass content of flying connections of iron converted to iron, %,no more than

0.00001

Test with permangate kally min not more than

60

Mass content of ammonia and amino compounds converted to ammonia, %, no more than

0.00001

Mass content of chlorine,%,no more than

0.0001

Mass content of sulphur, %, no more than

0.0001

Mass content of the non-volatile residue after evaporation,%,no more than

0.001

Specific conductivity the Ohm in (-1) sm in (-1)

3 x 10

Mass content 3tanona, % no more than

0.01

Chromaticity on a platino-cobalt scale of unit hazen, no more than

5

Purity wt %

: 99.0min

Colour Pt-Co (Hazen)

ASTM D 1364

: 15APHAmax

Water wt %

ASTM D 1364

: 0.1 max

Sp. Gr. at 20/20 o C

ASTM D 268

: 0.800-0.803

Distillation Range o C

ASTM D 1078

: 114-117

Acidity wt % ( As Acetic Acid )

ASTM D 1613

: 0.01 max

Molecular Weight

: 100.16

Boiling Point o C

: 116.2

Freezing Point C

: -84

Flash Point C

: 74

Evaporation rate ( o-buty acetate=1)

: 1.4

Water Miscibility

: 2.04

Explosive Limits ( Vol.% in air )

: 1.4-7.5

Refractive Index N o C

: 1.3958

Specific Heat Cal/g. o C

: 0.459

Viscosity cps at 20 o C

: 0.6

Appearance

SGS SPI 402-2

Clear and free from suspended matter

Colour PtCo

ASTM D 2108

<5

Nonvolatile matter, Method B

ASTM D 2109

mg/kg

<10

Water, Method A

ASTM D 3401

ppm

21

Acidity as HCI, procedure B

ASTM D 2989

ppm

0.6

Free Halogens

ASTM D 4755

Negative

Composition by GC

SGSSPI 016-1

Purity

SGSSPI 016-1

wt%

99.99

Amylene

SGSSPI 016-1

mg/kg

55

Other Chlorinated Hydrocarbons

SGSSPI 016-1

mg/kg

35

Density at 15 o C

ASTM D 4052

kg/L

1.3348

Appearance

in Flakes

Colour

White light yellow or light rose

Coloration is permissible

Crystallization temperature o C Min

79.6

Mass content of ash%Max

0.01

Crystallization point

o C

Min. 78.5

STPTC N2/79 BS 5962/80 (1993) ASTM D 1493-97

Ashos

%

Max. 0.05

ASTM D 482-95 STPTC CO 7/79BS 5962-80(1993)

Non volatile material

%

Max. 0.10

ASTM D 2232-81 BS 5962-80 STPTC N 6-79

Toluene insolubles

%

Max. 0.15

STPTC N 5/79 BS 144-97

Sulphur

%

Max. 0.60

ASTM D 5453-93 ASTM D 4629-96 ASTM D 5176-91

Water

%

Max. 0.1

ASTM D 95-83 (90)STPTC N 1/79

Purity

wt%

Min.99.9

100WT PCT-GC impurity WT PCT-HOWT PCT

99.96

Solidification

Min.40.7

ASTM D -1493

40.8

Carbonyl Compound

wt%

Max.0.007

ASTM E -411

0.003

Mesityl Oxide

wt%

Max.0.005

MV-71

0.0001

Water

wt%

Max.0.05

ASTM D-1631

0.02

Colour

Max.10

ASTM D-1209

5

Appearance

CLEAR

VISUAL

CLEAR

Appearance

White Crystal

Crystalization point, Min

40.6 o Centrigrade

Content of ( in dry Substance):

Phenol

99.0%min

Non volatile

0.008%max

Moisture content

No norms

Optical density of water solution of Phenol (8 gm) under 20 C, max

0.03

Optical density sulphurised Phenol, max

No norm

Colour of melted phenol at manufacturer, Hazen

No norm

Colour of melted phenol at buyer's place,Hazen

No norm

Mass content of Total Organic admixtures,% Max

No norm

Mass content of Organic admixtures,%Max

Meziethyl Oxide

0.004

Sum total of alphamethylstirol and Isopropylbenzol

0.01

Bulk Density 9/1.

500-750

Volatile Matter in percent max.

2

Sleve Analysis

NA

Total Alkalinity (as Na 2 CO 3 )% by mass min.

98.5

Matter insol in water % by mass max

0.15

Sulphate (as Na 2 SO 4 ) % By mass max.

0.08

Chloride (as NaCL) Percent by mass max

1.00

Iron (as Fe) percent by Mass max.

0.007

150 MIN
185 MAX

Sulfur Compound (H 2 S SO 2

ASTM D 853

NONE DETECTED

Acidity

MgnAOH/100ml

ASTM D 847

NO FREE ACID

Copper Corrosion

-

ASTM D 849

PASS (1A OR 1B)

Specific Gravity 15.6/15.6 ° c)

-

ASTM D 891

0-865- 0.880

Density @ 15 ° c( IN VAC)

G/ML

REPORT

Density @ 15 ° c( IN AIR)

G/ML

ASTM D 891

REPORT

Density @ 30 ° c( IN AIR

G/ML

ASTM D 891

REPORT

Color; Apha

-

ASTM D 1209

10MAX

Appearance

-

VISUAL

CLEAR

Appearance

Transparent homogeneous liquid without mechanical impurities and undissolved moisture

Styrene content,wt %, min

99,80

99,80

Phenylacetylene content, wt % max

0,01

-

Methylethylacrolein content, wt %, max

-

0,006

Divinyl benzene content, wt %, max

0,0005

-

Acetophenoze content, wt %,max

-

0,006

Carbonyl compounds (as benzaldehyde) content, wt, %, max

0,01

0,01

Peroxide compounds ( converted to active oxygen), wt, %, max

0,005

0,005

Polymer content, wt, %, max

0,001

0,001

Color, platinum-cobalt scale, Hazen, max

10

10

Stabilizer (para-tert-butylpyrocatechol) content, wt, %

0,0005-0,0010

0,0005-0,0010

Distillation Range

ASTM D 850

1.0 o C max. Including 110.6 o C

Appearance (@18-25 Deg C)

Visual

Bright & Clean, No residus

Total Non Aromatics

ASTM D 2360 modified

1.5 wt% max.

Color Pt-Cobalt

ASTM D 1209

20 max.

Copper Corrosion

ASTM D 849

1 max.

Density (@15 o C)

ASTM D 4052

0.869-0.873

Nonvolatile Residue

ASTM D 1353

 5 mg/100ml max

Acid Wash Color

ASTM D 848

2 max.

Benzene

ASTM D 2360 modified

0.1 wt%max.

Appearance

liquid is similar to distilled water in colour and transparency and includes no suspended matters

Density at 20G, g/cm

0,932-0,936

Distillate volume at 71,8-73 G, %,min

97

Mass fraction of acetaldehyde,%,max

0,025

Mass fraction of main substance,%,min

99,90

Mass fraction of croton aldehyde,%,max

None

Mass fraction of acid(in terms of acetic acid),%, max

0,005

Mass fraction of divinyl acetylene,% , max

0,0002

Mass fraction of water,%,max

0,05

Mass fraction of polyvinyl acetate

None

Molar viscosity of polyvinyl acetate in benzene, Pac(cp)min

0,035

Molar viscosity of polyvinyl acetate at 150+1 C on scale, max

1

Mass fraction of iron,5, max

0,00025